Preparation of high purity tellurium by zone refining

Preparation of Sulfur of High Purity

A mc thod is described for producing sulfur thaL conLains Ie. Lhan 1.3 X lO5 m ole [racLion of li q uid-solu ble, solid-insolubl e impuriLies as dcLermin ed by Lh e fr'eezing point depression . This corr e ponds t.o a purity of 99.999 mole p ercen t . Man y of Lhe impurities, including organic maLLcl', a r(' re moved by o,(ldaLion with s ulfuric and nitric ac ids. The nonvo lati le impuri ties ...

Preparation of High Purity Mullite Ceramics

Photolytic preparation of tellurium nanorods.

Well-defined tellurium nanorods have been prepared by the photolysis of (t)Bu2Te2 in an aqueous micellar system incorporating dodecanethiol as an auxiliary morphology-directing agent.

High-purity preparation of a large DNA dumbbell.

We report on the efficient biochemical synthesis of a large DNA dumbbell starting from a pair of short DNA hairpins with long single-stranded tails of arbitrary sequence. The DNA dumbbell is obtained by enzymatic ligation yielding a 94-bp duplex stem closed at both termini by single-stranded loops of 5 nt. Following ligation, all unligated precursors and monoligated by-products were multiply bi...

Laboratory for preparation of high-purity clinical chemicals.

A laboratory is described for the preparation and analysis of high-purity clinical chemicals. The work area is designed to minimize contact of high-purity materials with the main source of contamination, the chemical operator. We discuss the use of a perforated, curved, anodized aluminum membrane that permits completely free access to the work area and describe the general construction of the l...